Category Archives: Sample Preparation

Sample preparation of steel tanks.

 

Sometimes projects involve samples or artifacts too large or too valuable to remove or cut for evaluation in MEE’s laboratories. In these cases, in situ evaluation is required.

For this project, MEE was asked to evaluate the functional integrity of large steel tanks that had been exposed to elevated temperatures from a fire. Associate Engineer, Henry Ahrenholtz, is seen here preparing a field metallographic specimen. The tank surface was prepared by grinding, polishing and chemical etching to reveal the microstructure of the tank material. A replica of the prepared surface was made and then examined using a portable microscope. A Materials Engineer’s specialized knowledge of the material properties and behavior under certain environmental conditions combined with metallographic expertise in the field provided valuable information for the client to aid in assessing any damage to the tanks caused by fire.

 

 

To allow more consistent metallographic section preparation of very small targets, MEE has added a Leica EM/TXP to our selection of sectioning tools. The Leica EM/TXP is specifically designed for more precise and efficient targeting of points of interest in very small specimens. A combination mill/grinder/polisher and stereomicroscope, the Leica EM/TXP, allows the technician to observe the sample during preparation improving accuracy in locating microscopic targets.